Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 12, Pages 7901-7916Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b00706
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- Scientific and Technological Research Council of Turkey (TUBITAK) [315S049]
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Effective preparation of olivacine and ellipticine via late-stage D-ring cyclization is described. Key features of the synthetic routes include trifluoroacetic acid-mediated formation of a lactone that is fused to a tetrahydrocarbazole derivative and its one-pot two-step ring opening and aromatization mediated by para-toluenesulfonic acid and palladium on carbon, respectively.
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