Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 103, Issue -, Pages 87-92Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.inoche.2019.03.016
Keywords
Magnetic nanoparticles; Mn-Zn ferrite; Surface modification; Spectroscopy
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Funding
- Thailand Research Fund (TRF) through the Royal Golden Jubilee Ph.D. Program
- Center of Excellence in Materials Science and Technology, Chiang Mai University under the administration of Materials Science Research Center, Faculty of Science, Chiang Mai University (CMU), Thailand
- Graduate School of CMU
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One step hydrothermal synthesis of Mn-Zn ferrite was processed using different contents of ionic manganese, ionic zinc and oleic acid as an anti-agglomeration. In this research, magnetic nanoparticles are soft agglomeration and narrow size distribution. Oleic acid can promote anisotropic growth of particles. The modified Mn-Zn ferrite nanoparticles were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS) and thermogravimetric analysis (TGA). A vibrating sample magnetometer (VSM) certified that the modified nanoparticles showed the superparamagnetic properties.
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