Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 25, Issue 29, Pages 7177-7184Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201806092
Keywords
1,5-HAT; amination; electrosynthesis; flow electrolysis; pyrrolidines
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Funding
- King Abdullah University of Science and Technology (KAUST), Saudi Arabia, Office of Sponsored Research [URF/1/1974-04-01]
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A hydrogen atom transfer-directed electrochemical intramolecular C-H amination has been developed in which the N-radical species are generated at the anode, and the base required for the reaction is generated at the cathode. A broad range of valuable pyrrolidines were prepared in good yields and with high chemoselectivity. The reaction was easily scaled up in both batch and continuous flow systems.
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