Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 25, Issue 39, Pages 9174-9179Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201901418
Keywords
amides; biohybrid catalysts; dynamic kinetic resolution; heterogeneous catalysis; key cross-linked enzyme aggregates
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Funding
- Swedish Research Council [2016-03897] Funding Source: Swedish Research Council
- Vetenskapsrådet [2016-03897] Funding Source: Medline
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Herein, we report on the use a biohybrid catalyst consisting of palladium nanoparticles immobilized on cross-linked enzyme aggregates of lipase B of Candida antarctica (CalB CLEA) for the dynamic kinetic resolution (DKR) of benzylic amines. A set of amines were demonstrated to undergo an efficient DKR and the recyclability of the catalysts was studied. Extensive efforts to further elucidate the structure of the catalyst are presented.
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