Journal
CHEMISTRY LETTERS
Volume 48, Issue 7, Pages 715-717Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.190197
Keywords
Photocatalysis; Ketone; alpha,beta-Unsaturated carboxylic acid
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Funding
- CREST-JST, Program for Leading Graduate School Integrative Graduate Education and Research Program in Green Natural Science at Nagoya University
- WISE Program (Doctoral Program for Worldleading Innovative & Smart Education) Graduate Program of Transformative Chem-Bio Research at Nagoya University
- JSPS for Scientific Research
- JSPS
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A readily available thioxanthone derivative, 3,6-dimethoxy-9H-thioxanthen-9-one, has been utilized as an effective catalyst for the conjugate radical addition of 1,3-dioxolane to alpha,beta-unsaturated carboxylic acids under light irradiation. Based on the experimental observations, involvement of a radical generation process via a single-electron transfer (SET) has been proposed.
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