Journal
CARBOHYDRATE POLYMERS
Volume 212, Issue -, Pages 235-241Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2019.02.053
Keywords
Cellulose nanowhiskers; Silver nanoparticles; Hydrogen peroxide monitoring; Optical sensor; Colorimetric sensor
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Funding
- Fundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP) [2014/21184-5, 2017/12174-4, 2018/09414-6]
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq)
- MCTI-SisNano [CNPq/402.287/2013-4]
- Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior - Brasil (CAPES) [001]
- Rede Agronano (EMBRAPA) from Brazil
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Hydrogen peroxide (H2O2) is an important compound for several industrial sectors, but it becomes harmful to human health under high concentrations. Thus, the development of simple, low cost and fast analytical methods capable to detect and monitor H2O2 is fundamentally important. In the present study, we report a simple route for synthesizing silver nanoparticles (AgNPs) in the presence of a nanostructured polysaccharide (cellulose nanowhiskers) to produce a hybrid material, which was employed as a colorimetric probe for H2O2 detection. Our results revealed that AgNPs tend to experience catalytic decomposition when exposed to H2O2, causing a decrease of AgNPs absorption band at 410 nm in accordance with H2O2 concentration. This decrease was linearly dependent on H2O2 concentration (in the ranges 0.01-30 mu M and 60-600 mu M), yielding limits of detection of 0.014 mu M and 112 mu M, respectively. The easy-to-interpret H2O2 sensor also proved to be suitable for real samples analysis even in the presence of other interfering substances.
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