Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 55, Issue 8, Pages 2733-2737Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201510203
Keywords
chromatography; diffusion; analysis of mixtures; NMR spectroscopy; silica
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Funding
- Starting Grants Project MOSAIC [259014]
- PRAT CPDA [132473/13]
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The use of micrometric hollow silica spheres is described as a strategy to reduce magnetic field inhomogeneities in the context of NMR chromatography. When employed as a stationary phase, hollow silica microspheres allow the use of common solution-state NMR instruments to measure the diffusion coefficient perturbation induced by the interaction of the analytes with the silica surface.
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