Journal
ACS CATALYSIS
Volume 9, Issue 3, Pages 1630-1634Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acscatal.8b04633
Keywords
electrochemistry; nickel; Ullmann coupling C-S bond; metal catalysis; thiolation; arylation
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Funding
- National Natural Science Foundation of China [21472082, 21402088, 21772085]
- Fundamental Research Funds for the Central Universities [020514380148]
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This work describes a nickel-catalyzed Ullmann-type thiolation of aryl iodidesunder mild electrochemical conditions. The simple undivided cell with graphene/nickel foam electrode setups offers excellent substrate tolerance, affording aryl and alkyl sulfides in good chemical yields. Furthermore, the mechanism for this electrochemical cross-coupling reaction has been investigated by cyclic voltammetry.
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