Journal
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
Volume 111, Issue -, Pages 85-99Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.trac.2018.12.003
Keywords
Tetrabromobisphenol A; Derivatives; Transformation and degradation (T/D); Identification; Extraction; Purification; Mass spectrometry; Quantitative analysis
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Funding
- National Natural Science Foundation of China [21707148, 21527901]
- China Postdoctoral Science Foundation [2016M602210, 2018T110715]
- State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences [KF2016-12]
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The structural identification as well as quantitative analysis of transformation and degradation (T/D) products of tetrabromobisphenol A (TBBPA) and its derivatives can provide useful information on the corresponding T/D mechanism as well as environmental impact. However, it is still a great challenge to analyze trace levels of T/D products, both unknown and known products, as a result of the complexity of environmental matrices and the lack of commercial/artificial standard chemicals. This critical review summarized the T/D model experiments, sample preparation and the associated analytical methods, including extraction, purification, concentration, derivatization, quantitation analysis and C-14-labeling technologies. Furthermore, the mass spectral analysis of TBBPA related compounds using different analytical instruments and T/D products predicted by computer programs are also described. (C) 2018 Elsevier B.V. All rights reserved.
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