Journal
SEPARATION AND PURIFICATION TECHNOLOGY
Volume 211, Issue -, Pages 809-815Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.seppur.2018.10.045
Keywords
N-heterocyclic palladium complex; Fe3O4@SiO2; Reduction; Cr(VI); 4-NP
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Funding
- Iranian Nano Council
- University of Qom
- Iran National Science Foundation (INSF)
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In the present work, the organic palladium complex ((1-phenyl-1H-tetrazole-5-thiol)palladium(II)) was immobilized on the nano Fe3O4@SiO2 using (3-chloropropyl)trimethoxysilane. The [Fe3O4@SiO2-Tet-thio-Pd(II)] as a novel, efficient and reusable catalyst was fully characterized using different techniques such as FT-IR, XRD, FE-SEM, EDS, VSM, and TG-DTA. This heterogeneous catalytic system exhibited excellent activity in the catalytic reduction of Cr(VI) and 4-nitrophenol (4-NP) in aqueous media. The catalytic activities of the [Fe3O4@SiO2-Tet-thio-Pd(II)] in reactions were monitored by using UV Vis spectroscopy. Moreover, the catalyst could be recovered and reused five times without any remarkable loss of its catalytic activity.
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