Journal
ANALYTICAL METHODS
Volume 8, Issue 37, Pages 6815-6820Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ay01654e
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Funding
- French National Research Agency [ANR-12-JSV5-0005 (ANR33HRMACSZ)]
- JEOL RESONANCE Inc.
- TRAIL [ANR-10-LABX-57]
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This study evaluates the performances of a recently introduced 1 mm HR mu MAS NMR probe for metabolic profiling of nanoliter samples. It examines essential NMR criteria such as spectral data qualities and repeatability, and experimental practicality. The report also discusses the difficulties related to the sample preparation in HRmMAS experiments and considers possible solutions and improvements.
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