Journal
ORGANIC LETTERS
Volume 21, Issue 7, Pages 2269-2272Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b00558
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Funding
- National Natural Science Foundation of China [21302231]
- Hunan Provincial Natural Science Foundation of China [14JJ3021]
- Programs Foundation of Ministry of Education of China [20130162120032]
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A novel, efficient Z-alkene synthesis via photo-catalyzed decarboxylative couplings between terminal aryl alkynes and alkyl N-hydroxyphthalimide (NHPI) esters, which are derived from aliphatic carboxylic acids, is described. A wide range of primary, secondary, and tertiary carboxylates as well as alpha-amino acid and alpha-oxyacid-derived esters were employed as suitable substrates. The mild reaction conditions, broad substrate scope, functional group tolerance, and operational simplicity make this decarboxylative coupling reaction a valuable method in organic syntheses.
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