Journal
ORGANIC LETTERS
Volume 21, Issue 6, Pages 1939-1942Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b00706
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Funding
- DFG [ME 2756/9-1]
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The enantioselective total synthesis of (+)-salimabromide was accomplished by a concise two-step conversion of the fully functionalized dibromo-tetraline core, involving a one-pot Baeyer-Villiger/allylic oxidation by an innovative radical reagent combination. This route unequivocally resolves the stereochemistry and reveals the highly unusual, almost racemic nature of natural salimabromide.
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