Journal
ORGANIC LETTERS
Volume 21, Issue 6, Pages 1849-1852Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b00445
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Funding
- National Natural Science Foundation of China [21672141]
- Shanghai University
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An air-stable N,N'-dihydroporphycene, the two-electron reduced form of porphycene, possessing two quinoxaline moieties fused at meso positions, was prepared and characterized. Nuclear magnetic resonance (NMR) and ultraviolet-visible light (UV-vis) spectroscopic studies and single-crystal X-ray diffraction analyses support its formulation as a nonaromatic species. Upon treatment with tetrabutylammonium fluoride (TBAF) in chloroform, a color change is produced that is consistent with deprotonation. Selective detection of this anion is readily achieved.
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