Journal
ORGANIC LETTERS
Volume 21, Issue 4, Pages 1237-1240Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b00361
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Funding
- Guangzhou Education Bureau University Scientific Research Project [201831845]
- Talent Fund for High-Level University Construction of Guangzhou [B185006009007]
- National Natural Science Foundation of China [U1601227]
- Science and Technology Programs of Guangdong Province [2015B020225006]
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The catalyst-free electrochemical di- and trifluoromethylation/cyclization of N-substituted acrylamides was realized under external oxidant-free conditions. The strategy provides expedient access to fluoroalkylated oxindoles and 3,4-dihydroquinolin-2(1H)-ones with ample scope and broad functional group tolerance by mild, direct electrolysis of sodium sulfinates in an undivided cell. Detailed mechanistic studies provided strong support for a SET-based reaction manifold.
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