Journal
ANALYTICA CHIMICA ACTA
Volume 926, Issue -, Pages 28-35Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.aca.2016.04.010
Keywords
Reduced graphene oxide electrode; Functionalization; Ferrocene; Non-enzymatic sensor; Biosensor
Categories
Funding
- Severo Ochoa Program (MINECO) [SEV-2013-0295]
- MICINN [MAT2011-25870]
- Generalitat de Cataluna
- Ministry of Higher Education and Scientific Research of Tunisia (MHESR)
- UTM University
- LCAE Laboratory [LR99ES15]
- ICREA Funding Source: Custom
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A novel ferrocene-functionalized reduced graphene oxide (rGO)-based electrode is proposed. It was fabricated by the drop casting of ferrocene-functionalized graphene onto polyester substrate as the working electrode integrated within screen-printed reference and counter electrodes. The ferrocene-functionalized rGO has been fully characterized using FTIR, XPS, contact angle measurements, SEM and TEM microscopy, and cyclic voltammetry. The XPS and EDX analysis showed the presence of Fe element related to the introduced ferrocene groups, which is confirmed by a clear CV signal at ca. 0.25 V vs. Ag/AgCl (0.1 KCl). Mediated redox catalysis of H2O2 and bio-functionalization with glucose oxidase for glucose detection were achieved by the bioelectrode providing a proof for potential biosensing applications. (C) 2016 Elsevier B.V. All rights reserved.
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