Journal
JOURNAL OF SULFUR CHEMISTRY
Volume 40, Issue 3, Pages 256-264Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/17415993.2019.1570196
Keywords
Sulfonyl chlorides; sulfonamides; oxidative chlorination; chlorotrimethylsilane; hydrogen peroxide
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In this paper, a new method for oxidative chlorination of thiols to sulfonyl chlorides and sulfonamides using H2O2 in the presence of TMSCl is reported. The excellent yields, short reaction times, excellent efficiencies, low costs, and easy separation of products are the most important advantages of this method. [GRAPHICS] .
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