Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 5, Pages 2962-2968Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b02755
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Funding
- National Natural Science Foundation of China [21472056, 21772051, 21801022]
- Yangtze Youth Talents Fund [2016cqn25]
- Doctoral Scientific Research Startup Foundation of Yangtze University [801090010135]
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A trifluoroacetic acid (TFA)-mediated cascade oxidation/1,3-dipolar cycloaddition reaction of stabilized pyridinium salts with dimethyl sulfoxide (DMSO) has been developed in the presence of K2S2O8 and trimethylethylenediamine (TMEDA). In this transition-metal-free reaction, DMSO acts as a one-carbon source, thus providing a convenient method for the efficient and direct synthesis of various indolizine derivatives.
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