Journal
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
Volume 35, Issue 7, Pages 1412-1421Publisher
JOURNAL MATER SCI TECHNOL
DOI: 10.1016/j.jmst.2019.01.018
Keywords
Friction stir welding; Grain structure; Material flow; Pure copper
Funding
- New Energy and Industrial Technology Development Organization (NEDO)
- Japan Society for the Promotion of Science
- China Scholarship Council
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By employing a quasi in situ method, we investigated the dynamic evolution of the grain structure considering the material flow, strain, and strain rate in the friction stir welding of pure copper. The tool 'stop action' and rapid cooling were employed and a brass foil was used as a marker to show the material flow path. The grain structure along the material flow path was characterised using electron backscatter diffraction. Static recrystallization occurs for the work-hardened base material in the preheating stage in front of the tool. In the acceleration flow stage, grains are significantly refined by plastic deformation, discontinuous dynamic recrystallization, annealing twinning during the strain-induced boundary migration and slight continuous dynamic recrystallization. In the deceleration flow stage, due to a strain reversal, the grain first coarsens, and is thereafter refined again. Finally, the hot-deformed material in the shoulder-affected zone is 'frozen' directly whereas that in the probe-affected zone undergoes significant annealing; thus, the recrystallized microstructure and 45 degrees-rotated cube texture are obtained in the probe-affected zone. (C) 2019 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.
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