Journal
INORGANIC CHEMISTRY
Volume 58, Issue 5, Pages 3265-3270Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.inorgchem.8b03340
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Funding
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico, CNPq
- Fundacao de Amparo a Ciencia e Tecnologia de Pernambuco, PRONEX/FACEPE
- Coordenacao de Aperfeicoarnento de Pessoal de Nivel Superior, CAPES
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A luminescence quantum yield of 7.8% was obtained for a quaternary mixed-ligand samarium complex; this value is higher than those previously reported in the literature for such complexes in solution. The complex was prepared by microwave-assisted synthesis in 15 min with a yield of 69%; that is similar to 400 times faster than the usual synthesis that required 4 days and led to a yield of only 30%. Therefore, we propose microwave-assisted synthesis as the method of choice for preparing mixed-ligand lanthanoid complexes.
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