Journal
COMPOSITES PART B-ENGINEERING
Volume 160, Issue -, Pages 632-643Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.compositesb.2018.12.106
Keywords
PVDF-CNT membrane; Contact angle; XRD; FTIR; Raman; TGA; Tensile; Salt rejection
Funding
- 2017 Post-Doc. Development Program of Pusan National University
- Basic Science Research Program through the National Research Foundation of Korea (NRF) - Ministry of Education [2015R1D1A3A01019420]
- Creative Materials Discovery Program through the National Research Foundation of Korea (NRF) - Ministry of Science and ICT, South Korea [NRF-2017M3D1A1039287]
- Pusan National University, Busan, Korea
- National Research Foundation of Korea [2015R1D1A3A01019420] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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PVDF-CNT membranes were fabricated using thermally induced phase separation (TIPS) protocol. The membranes are extremely tensile, strong and robust. Membranes exhibit hydrophilic behavior with decreasing contact angle (CA < 90 degrees) in saline environment. Crystal study (XRD) of membranes reveals alpha-phased PVDF with hexagonal (002) oriented CNTs within the polymer matrix. The morphology (SEM) and thermal analysis (TGA) reveals that the material is made of several porous zones and the material is chemically and thermally stable up to 500 degrees C. Raman and FTIR spectrum shows ordered bands of the D and G with complete grafting of PVDF bonds with CNTs respectively.
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