Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 58, Issue 20, Pages 6742-6746Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201901902
Keywords
[3+3]-annulations; bicyclo[4,4,0]decanes; bicyclo[4,3,0]nonanes; organocatalysis; vinylogous reactivity
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Funding
- European Research Council under the European Union [277588]
- Greek General Secretariat of Research and Technology for matching (reward) funds [KA: 4143]
- Alexander S. Onassis Public Benefit Foundation [G ZM 063-1/2016-2017]
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A method for asymmetric and site selective annulations at the and positions of cyclic 2-enones with ,-unsaturated aldehydes has been developed. The organocatalysed [3+3]-annulations proceed with high levels of regio-, diastereo-, and enantioselectivity, affording a series of high value fused carbocycles. Further elaboration gave key lactones (both bridged and fused).
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