Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 361, Issue 12, Pages 2904-2915Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201900067
Keywords
Organophosphorus compounds; Phosphoryl thioamides; Willgerodt-Kindler reaction; Phosphinic Chlorides; Sulfur
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Funding
- Russian Science Foundation [18-73-00321]
- Russian Science Foundation [18-73-00321] Funding Source: Russian Science Foundation
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A straightforward, practical, and atom-economical three-component synthesis of phosphoryl thioamides from phosphinic chlorides, elemental sulfur, and aliphatic amines has been developed. The scope and limitations of this transformation have been investigated. This protocol is distinguished by metal- and organic solvent-free conditions, and high tolerance to various functional groups; it can be adapted for scaled-up synthesis.
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