Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 361, Issue 8, Pages 1808-1814Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201900157
Keywords
metal-free; thiosulfonate; sulfur dioxide; organosulfur compound; thiol
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Funding
- Natural Sciene Foundation of Shandong Province [ZR2016JL012]
- National Natural Science Foundation of China [21302110, 8 b.]
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A simple and catalyst-free strategy was developed for the synthesis of unsymmetrical thiosulfonates using readily available DABCO center dot(SO2)(2) as a solid and bench-stable sulfur dioxide surrogate. The corresponding thiosulfonates were obtained through a radical pathway with good functional group tolerance. This strategy offers a promising synthesis method for the construction of diverse and useful thiosulfonates in the field of synthetic and pharmaceutical chemistry and extends the number of still limited sulfur dioxide fixation strategies.
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