Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 358, Issue 20, Pages 3277-3282Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201600363
Keywords
deuterium; fatty acids; isopropyl alcohol; platinum on carbon; valproic acid
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Funding
- Research Foundation for Pharmaceutical Sciences
- JSPS [15J01556]
- Grants-in-Aid for Scientific Research [16K08169, 16K15100, 15J01556] Funding Source: KAKEN
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We have established a mild and direct platinum on carbon (Pt/C)-catalyzed multi-deuterium labeling of various saturated fatty acids including bioactive compounds with high deuterium efficiencies in a mixed solvent of isopropyl alcohol and deuterium oxide (i-PrOH)/D2O under neutral conditions at 120 degrees C without the external addition of deuterium or hydrogen gas.
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