Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 358, Issue 19, Pages 3135-3144Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201600350
Keywords
ball milling; O,N-dialkyl hydroxamates; hydroxamic acids; mechanochemical activation; mechanochemistry
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Funding
- Universita degli Studi di Cagliari [PRID 2015]
- Regione Autonoma della Sardegna [L.R. 7/2007, CUP F71J120001090002]
- Fondazione Banco di Sardegna [Prot. U875.2014/AI.758.MGB, Prat.2014. 0803]
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An operationally simple, and cost efficient conversion of carboxylic acids into hydroxamic acid derivatives via a high-energy mechanochemical activation is presented. This ball milling methodology was applied to a wide variety of carboxylic acids dramatically improving purification issues associated with this class of molecules, which still remain one of the main bottlenecks of classical methodologies.
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