Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 358, Issue 9, Pages 1410-1416Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201501183
Keywords
alkynes; continuous operation; formic acid; semireduction; supported gold nanoparticles
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Funding
- National Natural Science Foundation of China [21273044, 21473035, 91545108]
- Research Fund for the Doctoral Program of Higher Education [2012007000011]
- SINOPEC [X514005]
- Science & Technology Commission of Shanghai Municipality [08DZ2270500]
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A convenient and robust protocol for the selective transfer semireduction of alkynes was developed, using bio-renewable formic acid as the hydrogen source and easily handled supported gold nanoparticles as the catalyst. The catalytic system showed several attractive features such as high activity and selectivity, recyclability, scalability and adaptability to continuous operation under mild reaction conditions, thus providing a practical alternative to current methods for alkyne semireduction.
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