Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 358, Issue 23, Pages 3765-3769Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201601106
Keywords
azobenzenes; diboration; N-heterocyclic carbenes; palladium; silaboration
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Funding
- Royal Society of Chemistry (RSC)
- EPSRC Standard Research Student (DTG) [EP/L505109/1]
- Engineering and Physical Sciences Research Council [1366805] Funding Source: researchfish
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The bis(N-heterocyclic carbene)(diphenylacetylene)palladium complex [Pd(ITMe)(2)(PhCCPh)] (ITMe=1,3,4,5-tetramethylimidazol-2-ylidene) acts as a highly active pre-catalyst in the diboration and silaboration of azobenzenes to synthesize a series of novel functionalized hydrazines. The reactions proceed using commercially available diboranes and silaboranes under mild reaction conditions.
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