Journal
TETRAHEDRON LETTERS
Volume 59, Issue 49, Pages 4364-4369Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2018.10.067
Keywords
Cross dehydrogenative coupling; Photocatalysis; C-C bond formation; alpha-Aryla alpha-amino esters; Metal-free
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Funding
- National Natural Science Foundation of China [21606202, 21506190]
- College of Pharmaceutical Sciences, Zhejiang University of Technology
- Advanced Research Fund for the Doctoral Program of Zhejiang Province
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A novel photocatalytic cross dehydrogenative coupling reaction of N-aryl glycine esters with N-substituted anilines has been developed. The reaction proceeds effectively using methylene blue as a photocatalyst under visible light irradiation without any metal, chemical oxidant or additive. A variety of alpha-aryl alpha-amino derivatives were prepared in moderate to excellent yields with a high para-regioselectivity. (C) 2018 Elsevier Ltd. All rights reserved.
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