Journal
ORGANOMETALLICS
Volume 38, Issue 3, Pages 606-609Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.organomet.8b00840
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Funding
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences, Heavy Elements Chemistry Program [DE-SC0008479, DE-FG02-13ER16414]
- U.S. Department of Energy (DOE) [DE-SC0008479] Funding Source: U.S. Department of Energy (DOE)
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Anhydrous americium(III) starting materials were prepared from americia (AmO2) using inexpensive, commercially available reagents and mild reaction conditions. [AmCl(mu-Cl)(2)(THF)(2)](n) (1-Am) and AmBr3(THF)(4)(2-Am) were isolated and characterized by electronic absorption spectroscopy and X-ray diffraction. These new starting materials are soluble in organic solvents, making them useful synthons for nonaqueous organometallic americium chemistry.
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