Journal
ORGANIC LETTERS
Volume 21, Issue 3, Pages 618-622Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b03652
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Funding
- National Natural Science Foundation of China [21773273, 21473226]
- Key Research Program of Frontier Sciences, CAS [QYZDJ-SSW-SLH051]
- Natural Science Foundation of Jiangsu Province [BK20170420]
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A highly efficient strategy for the enantioselective oxidation of methylene C-H of spirocyclic oxindoles and dihydroquinolinones has been established, in which an earth-abundant manganese catalyst and hydrogen peroxide are used. Noteworthy, the manganese catalyst can be applied to the asymmetric hydroxylation of spirocyclic 2,3-dihydroquinolin-4-ones with 94-99% ee.
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