Journal
MENDELEEV COMMUNICATIONS
Volume 28, Issue 6, Pages 579-581Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.mencom.2018.11.004
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Diastereoselective synthesis of racemic and enantiopure 3-aryl-5-ethyl-1,4,2-oxazaphosphorines, including those bearing phenolic hydroxyl groups in the exocyclic aromatic fragment, was implemented by the reaction of imines derived from (+/-)- and (R)-(-)-2-aminobutan-1-ol and (hydroxy)benzaldehydes with triethyl phosphite and trifluoroacetic acid, followed by the one-pot dealkylation of the intermediate esters.
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