Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 2, Pages 1064-1069Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b02670
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Funding
- National Natural Science Foundation of China [21562025]
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An unprecedented method for cleaving the C=C bond in N,N-disubstituted enaminones in the presence of elemental sulfur and N,N-dimethyl-4-aminopyridine is disclosed. Without using any metal catalyst or additive, the cascade functionalization of both C=C and C-H bonds takes place to enable the formation of new C=S and C-N bonds, thus providing a facile and practical method for the synthesis of N,N-disubstituted alpha-keto thioamides.
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