Journal
CATALYSIS COMMUNICATIONS
Volume 118, Issue -, Pages 65-69Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2018.09.017
Keywords
Mechanochemistry; Aluminosilicate; Iron oxide; Vanillin
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Funding
- MINECO [CTQ2016-78289-P, REF BES-2017-081560, CTQ2016-78289]
- FEDER funds
- Sistan and Baluchestan University of Iran
- RUDN University Program 5-100
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A mechanochemical protocol was applied to the synthesis of a magnetic material based on iron oxide nano particles and Al-SBA-15. Full characterization of the prepared Fe2O3/Al-SBA-15 evidenced the effective functionalization of the ahuninosilicate surface. Particularly, TEM analysis revealed that the mechanochemical protocol did not considerable affect the hexagonal ordered structure of Al-SBA-15. DRIFT experiments of Fe2O3/Al-SBA-15 showed interesting acidic properties, which can be further associated to a good catalytic performance. The catalytic behavior of the prepared material was tested in the oxidation of vanillyl alcohol to vanillin, displaying an excellent activity and selectivity. The material resulted to be highly stable in the aforementioned reaction, without considerable decrease of conversion after 10 reuse cycles.
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