Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 15, Issue -, Pages 67-71Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.15.7
Keywords
carbene transfer; cyclopropane; cyclopropylcarboxylate; ethylene cyclopropanation; ethyl diazoacetate; gold catalysis
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Funding
- MINECO [CTQ2017-82893-C2-1-R, CTQ2015-73693-JIN]
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Ethylene can be directly converted into ethyl 1-cyclopropylcarboxylate upon reaction with ethyl diazoacetate (N2CHCO2Et, EDA) in the presence of catalytic amounts of IPrAuCl/NaBAr4F (IPr = 1,3-bis(2,6-diisopropylphenyl)imidazole-2-ylidene, BAr4F = tetrakis(3,5-bis(trifluoromethyl)phenyl)borate).
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