Journal
APPLIED ORGANOMETALLIC CHEMISTRY
Volume 32, Issue 12, Pages -Publisher
WILEY
DOI: 10.1002/aoc.4576
Keywords
Antimicrobial activities; Cyclic voltammetry; Imidazole; Spectroscopic behaviors; X-ray photoelectron spectrum
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Funding
- Fundamental Research Funds of the Gansu Province Universities [214152]
- Foundation of A Hundred Youth Talents Training Program of Lanzhou Jiaotong University [152022]
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Two two-dimensional and three-dimensional supramolecular complexes [M (L)(2)] (NO3)(2)center dot 2CH(3)OH (M = Cu(1) and Co(2), L = 2-(4-imidazolyl)-4-methyl-1,2-quinazoline-N-3-oxide), were synthesized and characterized by FT-IR and UV-Vis spectroscopy, as well as elemental analysis. The spectroscopic data of both complexes were compared with the ligand L. Both complexes were determined by X-ray single-crystal diffraction and display similar coordination geometry and have a 2:1 ligand-to-metal ratio. All the central M (II) atoms are hexa-coordinated with perfect octahedral geometries. In the crystal structures, complexes 1 and 2 form an infinite 1-D chain-like and 2-D, 3-D supramolecular frameworks. X-ray photoelectron spectrum (XPS) and thermal stability of 2 was investigated. Moreover, electrochemical properties and antimicrobial activities of both complexes were also studied.
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