4.2 Article

Effect of microwave power on phase, morphology, and photocatalytic properties of BiOIO3 nanostructure

Journal

JOURNAL OF THE AUSTRALIAN CERAMIC SOCIETY
Volume 55, Issue 2, Pages 501-506

Publisher

SPRINGER
DOI: 10.1007/s41779-018-0256-6

Keywords

Microwave-assisted synthesis; Bismuth-oxy-iodate; Photocatalysis

Funding

  1. Thailand Research Fund through the Royal Golden Jubilee Ph.D. Program
  2. Center of Excellence in Materials Science and Technology, Chiang Mai University under the administration of Materials Science Research Center, Faculty of Science, Chiang Mai University, Thailand

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Bismuth-oxy-iodate (BiOIO3) nanostructure was successfully synthesized by a microwave-assisted method. Phase, morphology, and optical properties of the as-synthesized products were characterized by XRD, SEM, TEM, FTIR, and UV-visible spectroscopy. In this research, the as-synthesized products were composed of orthorhombic BiOIO3 nanoplates. The Bi-O bending vibration showed a strong band at 513cm(-1) and I-O bending vibration showed as weak bands at 685 and 773cm(-1). The photocatalytic properties were evaluated through photodegradation of rhodamine B (RhB) induced by xenon visible radiation. The BiOIO3 nanoplates synthesized by 360W microwave for 60min with energy band gap of 2.75eV have the highest photocatalytic activity of 98.9% within 60min.

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