Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 1, Issue 3, Pages 294-297Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3qo00068k
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Funding
- National Basic Research Program of China [2012CB821600]
- Key Program of the Natural Science Foundation of China [21032006]
- National Natural Science Foundation of China [21172245, 21172244, 21372247]
- SIOC
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A new high yielding method for the preparation of a shelf-stable electrophilic trifluoromethylthiolating reagent, N-(trifluoromethylthio)phthalimide, is described. Reaction of this reagent with a variety of aryl and vinyl boronic acids in the presence of a copper catalyst generated the trifluoromethylthiolated arenes and alkenes in good to excellent yields.
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