4.5 Article

WO3 nanomaterials synthesized via a sol-gel method and calcination for use as a CO gas sensor

Journal

FRONTIERS OF CHEMICAL SCIENCE AND ENGINEERING
Volume 8, Issue 2, Pages 179-187

Publisher

SPRINGER
DOI: 10.1007/s11705-014-1431-0

Keywords

WO3 nanomaterial; sol-gel; calcinations; CO gas sensor; sensitivity

Funding

  1. Ministry of Research and Technology Republic of Indonesia [0161.12/IT2.7/PM/2012]
  2. Institut Teknologi Sepuluh Nopember (ITS)-Surabaya Indonesia [0750.042/I2.7/PM/2011]

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Carbon monoxide is a poisonous and hazardous gas and sensitive sensor devices are needed to prevent humans from being poisoned by this gas. A CO gas sensor has been prepared from WO3 synthesized by a sol-gel method. The sensor chip was prepared by a spin-coating technique which deposited a thin film of WO3 on an alumina substrate. The chip samples were then calcined at 300, 400, 500 or 600 degrees C for 1 h. The sensitivities of the different sensor chips for CO gas were determined by comparing the changes in electrical resistance in the absence and presence of 50 ppm of CO gas at 200 degrees C. The WO3 calcined at 500 degrees C had the highest sensitivity. The sensitivity of this sensor was also measured at CO concentrations of 100 ppm and 200 ppm and at operating temperatures of 30 and 100 degrees C. Thermogravimetric analysis of the WO3 calcined at 500 degrees C indicated that this sample had the highest gas adsorption capacity. This preliminary research has shown that WO3 can serve as a CO gas sensor and that is should be further explored and developed.

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