Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 2, Issue 3, Pages 259-264Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4qo00289j
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Funding
- Natural Science Foundation of China [21172162, 21372174]
- Young National Natural Science Foundation of China [21202111]
- Ph.D. Programs Foundation of Ministry of Education of China [2013201130004]
- Young Natural Science Foundation of Jiangsu Province [BK2012174]
- Key Laboratory of Organic Synthesis of Jiangsu Province [KJS1211]
- PAPD
- Soochow University
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A NIS/CHP-mediated [4 + 1]-cycloaddition of isocyanides with 1,2-diaza-1,3-dienes generated in situ from hydrazones under metal-free conditions has been developed. This protocol provides a new, atom efficient and step efficient way to construct aminopyrazoles in good to excellent yields via formation of new C-C/C-N bonds, utilizing a catalytic amount of NIS in the presence of CHP.
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