Journal
ADVANCED MATERIALS INTERFACES
Volume 5, Issue 20, Pages -Publisher
WILEY
DOI: 10.1002/admi.201801174
Keywords
honeycomb-patterned porous films; interfacial reactions; self-assembly; SnS thin layer
Funding
- National Research Foundation of Korea [2016-R1D1A1B03930614]
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A new fabrication process for the pore-selective functionalization of honeycomb-patterned porous (HCP) films is demonstrated by a modified breath figure method accompanied by an in situ chemical reaction. A polymer solution containing one reactant is cast under humid conditions containing counter reactant to facilitate a chemical reaction at condensed droplet/polymer solution interface, which results in the pore-selective functionalization of HCP films. Polystyrene (PS) solution containing tin(II) chloride is cast under humid conditions containing aqueous hydrogen sulfide for the formation of tin sulfide (SnS)-functionalized PS HCP films. H2S humidity is generated by pumping ambient air through the aqueous sodium sulfide solution. Scanning electron microscopy, transmission electron microscopy, and elemental mapping analyses indicate the formation of SnS as thin layers selectively in the pores of PS HCP films.
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