Journal
JOURNAL OF MATERIALS CHEMISTRY A
Volume 1, Issue 2, Pages 367-373Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ta00084a
Keywords
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Funding
- Innovation Program of Shanghai Municipal Education Commission [10YZ03, 10YZ05, 12YZ013]
- Science and Technology Committee [10DZ0500100, 11DZ110020]
- Natural Science Foundation of Shanghai [10ZR1411300]
- Shanghai Key Laboratory of Green Chemistry and Chemical Processes (ECNU)
- Laboratory of Chemical Engineering (ECUST)
- Shanghai Leading Academic Discipline Project [S30109]
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In this paper, a leaf-like porous CuO-graphene nanostructure is synthesized by a hydrothermal method. The as-prepared composite is characterized using XRD, Raman, SEM, TEM and nitrogen adsorption-desorption. The growth mechanism is discussed by monitoring the early growth stages. It is shown that the CuO nanoleaves are formed through oriented attachment of tiny Cu(OH)(2) nanowires. Electrochemical characterization demonstrates that the leaf-like CuO-graphene are capable of delivering specific capacitances of 331.9 and 305 F g(-1) at current densities of 0.6 and 2 A g(-1), respectively. A capacity retention of 95.1% can be maintained after 1000 continuous charge-discharge cycles, which may be attributed to the improvement of electrical contact by graphene and mechanical stability by the layer-by-layer structure. The method provides a facile and straightforward approach to synthesize CuO nanosheets on graphene and may be readily extended to the preparation of other classes of hybrids based on graphene sheets for technological applications.
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