Journal
JOURNAL OF MATERIALS CHEMISTRY A
Volume 1, Issue 9, Pages 2974-2977Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ta10239d
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Funding
- Research Council of Norway
- US Department of Energy, Office of Energy Efficiency and Renewable Energy
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Al-27 and Li-7 wide-line NMR spectroscopy incorporating a high pressure NMR apparatus has allowed the first in situ study of the solvent mediated, direct synthesis of an alanate, thus overcoming the dearth of analytical techniques available to study phenomena occurring in a pressurised slurry. In contrast to the decomposition reaction, the elucidated hydrogenation pathway does not proceed through the hexahydride intermediate.
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