Journal
JOURNAL OF MATERIALS CHEMISTRY A
Volume 1, Issue 21, Pages 6489-6496Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ta10472a
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Funding
- JSPS KAKENHI [23760679]
- Grants-in-Aid for Scientific Research [23760679] Funding Source: KAKEN
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Photocatalytic activity of graphitic carbon nitride (g-C3N4) was significantly improved by an alkaline hydrothermal treatment. The specific surface area of g-C3N4 obtained by heating melamine at 550 degrees C was only 7.7 m(2) g(-1), which was too small for it to be utilized as a catalyst for air purification. By the hydrothermal treatment with NaOH solution at 90-150 degrees C, the surface area was increased up to 65 m(2) g(-1), and the oxidation rate of nitrogen oxide (NO) under visible light (380 < lambda < 480 nm) was increased by 8.6 times. XRD, ESR, elemental analysis and electron microscopy showed that unstable domains of not-well-ordered carbon nitride were removed by hydrolysis to form a mesoporous structure with a higher surface area. Deactivation of g-C3N4 was not observed during the experimental period, although a small part of carbon nitride was decomposed by self-oxidation.
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