4.5 Article

Silver-Catalyzed Decarboxylative Trifluoromethylthiolation of Cinnamic Acids: An Easy Access to α-Trifluoromethylthiolated Ketones

Journal

ASIAN JOURNAL OF ORGANIC CHEMISTRY
Volume 7, Issue 9, Pages 1835-1838

Publisher

WILEY-V C H VERLAG GMBH
DOI: 10.1002/ajoc.201800327

Keywords

C-H activation; cross-coupling; synthetic methods; alpha-trifluoromethylthiolated ketones; decarboxylative difunctionalization

Funding

  1. SERB, New Delhi [EMR/2016/000750]
  2. UGC, New Delhi

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A silver-catalyzed decarboxylative difunctionalization of cinnamic acids has been developed to afford a variety of alpha-trifluoromethylthiolated ketones under mild reaction conditions using insitu generated SCF3 source by the combination of Langlois' reagent and CS2.

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