Journal
ASIAN JOURNAL OF ORGANIC CHEMISTRY
Volume 3, Issue 4, Pages 437-441Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ajoc.201402001
Keywords
4-dimethylaminopyridine; ketones; Morita-Baylis-Hillman reaction; nucleophilic catalysts; thioureas
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Funding
- JSPS KAKENHI [25870458]
- MEXT (Japan)
- Grants-in-Aid for Scientific Research [25410117, 25410042, 26105740, 24106730, 25870458] Funding Source: KAKEN
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The rate of the intramolecular Morita-Baylis-Hillman (MBH) reaction is remarkably enhanced by the combination of catalytic amounts of a nucleophilic catalyst (4-dimethylaminopyridine (DMAP), 4-pyrrolidinopyridine (PPY), or PBu3) and 1,3-diphenyl-2-thiourea, and the desired MBH adducts are obtained in good to high yields within a few hours.
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