Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 11, Issue -, Pages -Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.11.130
Keywords
4-acryloyloxy-2,2,6,6-tetramethylpiperidine-1-oxyl; cinnamates; Mizoroki-Heck cross-coupling reaction; nitroxides
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Funding
- Polish Ministry of Science and Higher Education [429/E-142/S/2012]
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Cinnamic acid derivatives bearing a nitroxyl moiety (2,2,6,6-tetramethyl-1-oxyl-4-piperidyl 3-E-aryl acrylates) were synthesized in 30-100% yield using a Mizoroki-Heck cross-coupling reaction between 4-acryloyloxy-2,2,6,6-tetramethylpiperidine-1-oxyl and iodobenzene derivatives in the presence of palladium(II) acetate coordinated with a tri(o-tolyl) phosphine ligand immobilized in a polyurea matrix.
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