Journal
JOURNAL OF FLOW CHEMISTRY
Volume 4, Issue 3, Pages 135-139Publisher
AKADEMIAI KIADO RT
DOI: 10.1556/JFC-D-14-00020
Keywords
Knoevenagel condensation; nitroaldol condensation; piperazine catalysis; microreactor; coumarin synthesis; polymer brushes
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- NanoNext NL
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The covalent attachment of piperazine onto the inner walls of a microreactor using glycidyl methacrylate polymer brushes has been demonstrated. The piperazine-containing polymer brushes were first grown on a flat silicon oxide surface and were characterized by contact angle, Fourier transform infrared (FT-IR), ellipsometry, and X-ray photoelectron spectroscopy (XPS). The applicability of the catalytic polymer brushes in a microreactor was demonstrated for the Knoevenagel and nitroaldol condensation reactions, and the synthesis of coumarin derivatives. The catalytic activity of the microreactor was still intact even after 2 months.
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