Journal
JOURNAL OF FLOW CHEMISTRY
Volume 2, Issue 3, Pages 70-+Publisher
SPRINGER
DOI: 10.1556/JFC-D-12-00004
Keywords
flow microreactor; vinyllithium
Categories
Funding
- Grant-in-Aid for Scientific Research
- Grants-in-Aid for Scientific Research [21106001, 21106002] Funding Source: KAKEN
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Vinyllithiums were effectively generated by bromine-lithium exchange reaction of vinyl bromides with one eq of s-BuLi in a flow microreactor system at 0 degrees C or 20 degrees C, although two eq of t-BuLi and much lower temperatures are required for a conventional macro batch reaction. Subsequent reactions with various electrophiles in the flow microreactor system gave the corresponding vinyl compounds in good yields.
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