Journal
JOURNAL OF THE CHILEAN CHEMICAL SOCIETY
Volume 57, Issue 1, Pages 1012-1016Publisher
SOC CHILENA QUIMICA
DOI: 10.4067/S0717-97072012000100013
Keywords
Lewis Acids; Dihydropyrimidinones; Biginelli condensation; Grindstone technique; SnCl4 center dot 5H(2)O
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Funding
- FET
- MITS
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A simple and efficient procedure for the one pot Biginelli Condensation Reaction of aldehydes, (beta-ketoester and urea employing SnCl4 center dot 5H(2)O /mono/di/tri-butyl-tin chloride as a novel catalyst is described. Compared to classical Biginelli reaction conditions, the present method has the advantages of good yields, short reaction times and experimental simplicity. Further, comparative efficiency of alkyl- tin chlorides in multicomponent Biginelli Condensation Reaction is also studied under solvent free conditions.
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